Posted by Piscean on Thursday, December 02, 2010
Product details
- Hardcover: 424 pages
- Publisher: CRC Press; 1 edition (11 Dec 1989)
- Language English
- ISBN-10: 0824781368
- ISBN-13: 978-0824781361
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Posted by Piscean on Thursday, December 02, 2010
Product Description
Includes new derivatizing reagents not covered in similar book by Blau and
Halket (Wiley 1993) and not found in any other books to date.
A field of increasing importance and significance in separation science.
Concentrates on synthesis of derivatives for HPLC and Capillary
Electrophoresis, techniques of great interest in the pharmaceutical field.
Product Details
- Hardcover: 312 pages
- Publisher: Wiley; 1 edition (March 31, 1999)
- Language: English
- ISBN-10: 0471983640
- ISBN-13: 978-0471983644
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Posted by Piscean on Sunday, November 28, 2010
Posted by Piscean on Monday, November 22, 2010
Posted by Piscean on Sunday, November 21, 2010
Review
"...should significantly enhance...understanding of the selected topic..." (THES Textbook Guide, 27 Feb 2004)
Product Description
First explaining the basic principles of liquid chromatography and
mass spectrometry and then discussing the current applications and
practical benefits of LC-MS, along with descriptions of the basic
instrumentation, this title will prove to be the indispensable reference
source for everyone wishing to use this increasingly important tandem
technique.
- First book to concentrate on principles of LC-MS
- Explains principles of mass spectrometry and chromatography before moving on to LC-MS
- Describes instrumental aspects of LC-MS
- Discusses current applications of LC-MS and shows benefits of using this technique in practice
Product Details
- Paperback: 296 pages
- Publisher: Wiley; 1 edition (April 11, 2003)
- Language: English
- ISBN-10: 0471498017
- ISBN-13: 978-0471498018
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Posted by Piscean on Wednesday, November 17, 2010
Posted by Piscean on Wednesday, November 17, 2010
Product Description
High-performance liquid chromatography (HPLC) is a procedure for
separating components from a mixture of chemical substances; a
combination of separation, identification, and quantitative
measurements. Solvent selection is perhaps the most commonly overlooked
parameter in HPLC. Even the most experienced analytical chemist tends to
select one of three familiar solvents.
The HPLC Solvent Guide provides detailed coverage of all commonly used HPLC solvents used in a wide range of separations.
HPLC is a mature but substantial market, and one that Wiley reaches
successfully and well. The HPLC list is established, and this second
edition of a successful title will build upon the success of the first.
This is a revised and expanded edition in a field that is still growing
into areas of analysis and methods.
Product Details
- Hardcover: 664 pages
- Publisher: Wiley; 2 edition (February 27, 2002)
- Language: English
- ISBN-10: 0471411388
- ISBN-13: 978-0471411383
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Posted by Piscean on Wednesday, November 17, 2010
Product Description
The only reference to provide both current and thorough coverage of this important analytical technique
Static headspace-gas chromatography (HS-GC) is an indispensable
technique for analyzing volatile organic compounds, enabling the analyst
to assay a variety of sample matrices while avoiding the costly and
time-consuming preparation involved with traditional GC.
Static Headspace-Gas Chromatography: Theory and Practice has long been
the only reference to provide in-depth coverage of this method of
analysis. The Second Edition has been thoroughly updated to reflect the
most recent developments and practices, and also includes coverage of
solid-phase microextraction (SPME) and the purge-and-trap technique.
Chapters cover:
* Principles of static and dynamic headspace
analysis, including the evolution of HS-GC methods and regulatory
methods using static HS-GC
* Basic theory of headspace
analysis-physicochemical relationships, sensitivity, and the principles
of multiple headspace extraction
* HS-GC techniques-vials, cleaning, caps, sample volume, enrichment, and cryogenic techniques
* Sample handling
* Cryogenic HS-GC
* Method development in HS-GC
* Nonequilibrium static headspace analysis
* Determination of physicochemical functions such as vapor pressures, activity coefficients, and more
Comprehensive and focused, Static Headspace-Gas Chromatography,
Second Edition provides an excellent resource to help the reader achieve
optimal chromatographic results. Practical examples with original data
help readers to master determinations in a wide variety of areas, such
as forensic, environmental, pharmaceutical, and industrial applications.
Product Details
- Hardcover: 376 pages
- Publisher: Wiley-Interscience; 2 edition (May 5, 2006)
- Language: English
- ISBN-10: 0471749443
- ISBN-13: 978-0471749448
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Posted by Piscean on Wednesday, November 17, 2010
Review
U.A. Th. Brinkman
Much useful information is provided for a wide range of readers.
THE ANALYST
Product Description
Sample preparation is an essential step in many analyses. This book
approaches the topic of sample preparation in chromatography in a
methodical way, viewing it as a logical connection between sample
collection and analytical chromatography. Providing a guide for choosing
the appropriate sample preparation for a given analysis, this book
describes various ways to process the sample, explaining the principle,
discussing the advantages and disadvantages, describing the
applicability to different types of samples, and showing the fitness to
specific chromatographic determinations.
The first part of the
book contains an overview of sample preparation showing its relation to
sample collection and to the core chromatographic analysis. The second
part covers procedures that do not use chemical modifications of the
analyte and includes methods for sample dissolution, concentration and
cleanup designed mainly for modifying the initial matrix of the sample.
This part starts with conventional separations such as filtration and
distillation and finishes with more advanced techniques such as solid
phase extraction and electroseparations. The third part gives a
description of the chemical modifications that can be performed on a
sample either for fractionation purposes or to improve a specific
property of the analyte. This part includes derivatizations, polymer
chemical degradations, and pyrolysis.
Product Details
- Hardcover: 942 pages
- Publisher: Elsevier Science; 1 edition (May 22, 2002)
- Language: English
- ISBN-10: 0444503943
- ISBN-13: 978-0444503947
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Posted by Piscean on Wednesday, November 17, 2010
Product Description
This revision brings the reader completely up to date on the evolving
methods associated with increasingly more complex sample types analyzed
using high-performance liquid chromatography, or HPLC. The book also
incorporates updated discussions of many of the fundamental components
of HPLC systems and practical issues associated with the use of this
analytical method. This edition includes new or expanded treatments of
sample preparation, computer assisted method development, as well as
biochemical samples, and chiral separations.
From the Publisher
This revision brings the reader completely up to date on the evolving
methods associated with increasingly more complex sample types analyzed
using high-performance liquid chromatography, or HPLC. The book also
incorporates updated discussions of many of the fundamental components
of HPLC systems and practical issues associated with the use of this
analytical method. This edition includes new or expanded treatments of
sample preparation, computer assisted method development, as well as
biochemical samples, and chiral separations.
Product Details
- Hardcover: 765 pages
- Publisher: Wiley-Interscience; 2nd edition (March 3, 1997)
- Language: English
- ISBN-10: 047100703X
- ISBN-13: 978-0471007036
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Posted by Piscean on Wednesday, November 17, 2010
Product Description
This book gives a comprehensive overview of the basis and the current
applications of LC-NMR and related techniques. It deals with the
practical aspects of the hardware and software set-up for a successful
performance of on-line coupling experiments. It covers the solution of
real-word problems from the fields of biomedical, pharmaceutical and
environmental studies as well as the analysis of natural products and
polymeric compounds. Thus guidelines for an efficient application of the
powerful hyphenated technique LC-NMR in combination with LC-MS are
presented. Besides LC-NMR, important techniques such as the on-line
coupling of gel permeation chromatography and supercritical fluid
chromatography, together with 1H NMR spectroscopy, are described in
detail. Fascinating further aspects, such as the application of
capillary separation techniques either in the single or parallel
detection mode, together with the possibilities of direct 13C monitoring
of chromatographic events, are also discussed.
Key features include:
- Up-to-date information on the theoretical and experimental methodology
-
Coverage of applications in biomedical, pharmaceutical and natural
product analysis, as well as environmental polymer and related
hyphenated techniques
- Information appropriate for researchers in organic, pharmaceutical and medical chemistry
Overall, this book is a requirement for all researchers and staff
members dealing with structure elucidation problems in separation
science.
Product Details
- Hardcover: 306 pages
- Publisher: Wiley (September 17, 2002)
- Language: English
- ISBN-10: 0471496499
- ISBN-13: 978-0471496496
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Posted by Piscean on Wednesday, November 17, 2010
Product Description
The bible of gas chromatography--offering everything the professional
and the novice need to know about running, maintaining, and interpreting
the results from GC Analytical chemists, technicians, and
scientists in allied disciplines have come to regard Modern Practice of
Gas Chomatography as the standard reference in gas chromatography. In
addition to serving as an invaluable reference for the experienced
practitioner, this bestselling work provides the beginner with a solid
understanding of gas chromatographic theory and basic techniques.
This
new Fourth Edition incorporates the most recent developments in the
field, including entirely new chapters on gas chromatography/mass
spectrometry (GC/MS); optimization of separations and computer
assistance; high speed or fast gas chromatography; mobile phase
requirements: gas system requirements and sample preparation techniques;
qualitative and quantitative analysis by GC; updated information on
detectors; validation and QA/QC of chromatographic methods; and useful
hints for good gas chromatography.
As in previous editions,
contributing authors have been chosen for their expertise and active
participation in their respective areas. Modern Practice of Gas
Chromatography, Fourth Edition presents a well-rounded and comprehensive
overview of the current state of this important technology, providing a
practical reference that will greatly appeal to both experienced
chomatographers and novices.
Product Details
- Hardcover: 1064 pages
- Publisher: Wiley-Interscience; 4 edition (June 11, 2004)
- Language: English
- ISBN-10: 0471229830
- ISBN-13: 978-0471229834
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Posted by Piscean on Wednesday, November 17, 2010
Review
FROM THE REVIEWS:
JOURNAL OF THE AMERICAN CHEMICAL SOCIETY
"In
summary, the book presents an important overview of seven emerging
chromatographic/separation methodologies and strategies that will have a
significant impact on solving many problems faced in the field of
biotechnology. The presentation is of high quality, encompassing, and is
well suited for separation specialists in biotechnology and also in
other areas where separations play a key role.”
Product Description
Chromatography is the separation method for biological molecules from
the analytical to the preparative scale. Few of the recent advances in
life science, whether in "proteomics" or in the industrial production of
recombinant therapeutics, would have been possible without the help of
chromatographic separations. Concomitantly, chromatography nowadays
stands for much more than a batch column packed with porous particles.
In this book eminent experts from academia and industry introduce the
reader to some of the recent new developments in this exciting area.
Ranging from evolving nanoanalytical techniques to advances in the
material sciences and artificial antibodies and finally continuous large
scale separations of the most fragile biologicals, this book should
provide interesting reading material for students and practitioners from
various fields.
Product Details
- Paperback: 271 pages
- Publisher: Springer; 1st Edition. edition (November 2, 2010)
- Language: English
- ISBN-10: 3642077064
- ISBN-13: 978-3642077067
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Posted by Piscean on Wednesday, November 17, 2010
Review
"&a comprehensive primer and will appeal to laboratory scientists and instructors in the pharmaceutical field&" --
Analytical Chemistry, November 2002"...describes...applications
in each phase of drug development...provides perspective on changes in
strategies for pharmaceutical analysis..." --
SciTech Book News, Vol. 26, No. 2, June 2002
Product Description
Breakthroughs in combinatorial chemistry and molecular biology, as
well as an overall industry trend toward accelerated development, mean
the rate of sample generation now far exceeds the rate of sample
analysis in the pursuit of producing new and better pharmaceuticals.
LC/MS is an analytical tool that helps the researcher identify the most
promising sample early in the selection process, effectively creating a
shortcut to finding new drugs. This book is the first to describe LC/MS
applications within the context of drug development, including the
discovery, preclinical, clinical, and manufacturing phases.
In
addition to the thorough technical analysis of this tool, LC/MS
Applications in Drug Development provides perspective on the significant
changes in strategies for pharmaceutical analysis. A process overview
of drug development from an analytical point of view is provided along
with essential data required to successfully bring a drug to market. The
incorporation of LC/MS is illustrated from target to product. Chapters
pertaining to the discovery process itself include: -Proteomics
-Glycoprotein Mapping
-Natural Products Dereplication
-Lead Identification Screening
-Open-Access LC/MS
-In Vitro Drug Screening
Written for both the analytical chemist who uses LC/MS applications
and the pharmaceutical scientist who works with the drugs they produce,
LC/MS Applications in Drug Development is the premier reference on the
subject.
Product Details
- Hardcover: 256 pages
- Publisher: Wiley-Interscience; 1 edition (March 7, 2002)
- Language: English
- ISBN-10: 0471405205
- ISBN-13: 978-0471405207
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Posted by Piscean on Wednesday, November 17, 2010
Posted by Piscean on Wednesday, November 17, 2010
Posted by Piscean on Wednesday, November 17, 2010
Posted by Piscean on Wednesday, November 17, 2010
Posted by Piscean on Wednesday, November 17, 2010
Product Description
This Second Edition of the classic handbook details how to set up an
HPLC system that capitalizes on the latest innovations. It covers new
techniques in high-temperature, micro-flow, and ultra-fast
chromatography, the linking of an HPLC to a mass spectrometer, and more.
Complete with a CD-ROM and appendices, this guide has everything
chromatographers need to know to confidently separate, identify, purify,
and quantify compounds.
Note: CD-ROM/DVD and other supplementary materials are not included as part of eBook file.
From the Publisher
Based on 15 years of laboratory and field conditions troubleshooting,
this essential and proven training manual for setting up and running an
HPLC system explains the underlying principles and provides methods for
starting up and maintaining HPLC systems. Five appendices including a
programmed self-learning guide, a guide to separations, a series of
laboratory experiments, and a glossary of terms make this book a must
for every chromatographer.
--This text refers to an out of print or unavailable edition of this title.
Product Details
- Hardcover: 256 pages
- Publisher: Wiley-Interscience; 2 edition (December 18, 2006)
- Language: English
- ISBN-10: 0471754013
- ISBN-13: 978-0471754015
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Posted by Piscean on Wednesday, November 17, 2010
Product Description
Gradient elution demystified
Of the various ways in
which chromatography is applied today, few have been as misunderstood as
the technique of gradient elution, which presents many challenges
compared to isocratic separation. When properly explained, however,
gradient elution can be less difficult to understand and much easier to
use than often assumed.
Written by two well-known
authorities in liquid chromatography, High-Performance Gradient Elution:
The Practical Application of the Linear-Solvent-Strength Model takes
the mystery out of the practice of gradient elution and helps remove
barriers to the practical application of this important separation
technique. The book presents a systematic approach to the current
understanding of gradient elution, describing theory, methodology, and
applications across many of the fields that use liquid chromatography as
a primary analytical tool.
This up-to-date, practical, and comprehensive treatment of gradient elution:
* Provides specific, step-by-step recommendations for developing a gradient separation for any sample
* Describes the best approach for troubleshooting problems with gradient methods
* Guides the reader on the equipment used for gradient elution
* Lists which conditions should be varied first during method development, and explains how to interpret scouting gradients
* Explains how to avoid problems in transferring gradient methods
With a focus on the use of linear solvent strength (LSS) theory for
predicting gradient LC behavior and separations by reversed-phase HPLC,
High-Performance Gradient Elution gives every chromatographer access to
this useful tool.
Product Details
- Hardcover: 496 pages
- Publisher: Wiley-Interscience (December 11, 2006)
- Language: English
- ISBN-10: 0471706469
- ISBN-13: 978-0471706465
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